Compounds of Arsenic, Antimony, and Bismuth: Covering the by Michael Dub (auth.), Michael Dub (eds.)

By Michael Dub (auth.), Michael Dub (eds.)

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Extra info for Compounds of Arsenic, Antimony, and Bismuth: Covering the Literature from 1965 to 1968

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The rate of the CO displacement by Ars was followed by IR spectroscopy and the rxn. mechanism was considered (643). Likewise, the rxn. 2 0 were followed by IR spectroscopy. Even at a Mo(CO)e:Ars ratio of 1:10 extremely limited disubstitution occurred; a SNl dissocn. mechanism was postulated (1599). The inductive effect of the ligand-metal a-bond and ligand-metal n-bond on the CO stretching force const. is considered (644). Spectra: IR (435, 439), electronic (439). Low-frequency IR spectrum; a tetragonal bipyramidal configuration with the Ars ligand in one of the apical pOSitions postulated (1419).

Prepd. from [(PrCN)2Mo]Ci4 + Ars in CHC13. Visible reflectance spectrum and magnetic susceptibility data; a 6-coordination of Mo postulated (58). [Mo(Ars)(CO)5] (M-23), prepd. from Mo(CO)e + Ars in decalin at 112°. The rate of the CO displacement by Ars was followed by IR spectroscopy and the rxn. mechanism was considered (643). Likewise, the rxn. 2 0 were followed by IR spectroscopy. Even at a Mo(CO)e:Ars ratio of 1:10 extremely limited disubstitution occurred; a SNl dissocn. mechanism was postulated (1599).

5-188°, prepd. 2 from [COS4C4(CF4)4J2 + Ars in dry C5H~2' Polarographic data, electronic and ESR spectra; a square-pyramidal structure for the 5-coordinate Co was suggested (110). [Co(Ars) [ON=C(Me)C(Me)=NOBPh2]2} , red-brown crystals, m. 192-195°, prepd. from {Co(Ars)[ON=C(Me)C(Me)=NOH]2Cl} in THF by treating the soln. with K (1:2) under reflux, followed by Ph2BCl and completing the rxn. under reflux. A structure with 4 N and As atoms chelated with the 5-coordinate Co was postulated (1350). [Ph2BCo(Ars) [ON=C(Me)C (Me)=NOBPh2]2} , brown crystals, prepd.

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